Optimization of Pesticide Analysis Method for Diazinon and Chlorantraniliprol Using High Performance Liquid Chromatography (HPLC)

Marselina Theresia Djue Tea, Akhmad Sabarudin, Hermin Sulistyarti

Abstract


Metode penetuan diazinon dan klorantraniliprol dalam sampel tanah telah dikembangkan. Analit diekstrak menggunakan asetonitril dengan menggunakan metode ultrasonic solvent extraction (USE). Penetuannya menggunakan kromatografi cair kinerja tinggi menggunakan detektor UV. Kondisi optimum untuk pemisahan kedua pestisida adalah komposisi Asetonitril:Air (60:40), laju alir 0,4 mL/min, dan pada panjang gelombang 220 nm. Semakin banyak jumlah asetonitril dalam campuran eluen maka waktu retensi senyawa dalam kolom semakin cepat. Waktu retensi masing-masing senyawa, klorantraniliprol 10.525, dan diazinon 21.029.


Keywords


KCKT, Pestisida, Diazinin, Klorantraniliprol

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References


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